Журналы →  Tsvetnye Metally →  2022 →  №2 →  Назад

HYDROMETALLURGY
Название Developing a regeneration process for ceramic elements of vacuum filters in operation at the copper concentrate filtration station of Copper Plant
DOI 10.17580/tsm.2022.02.08
Автор Efimov A. A., Bolshakova O. V., Glibovets M. V., Midyukov D. O.
Информация об авторе

MMC Norilsk Nickel’s Polar Division, Norilsk, Russia:

A. A. Efimov, Director of the Engineering Support Centre, e-mail: EfimovAA@nornik.ru
O. V. Bolshakova, Head of the Laboratory at the Engineering Support Centre, e-mail: BolshakovaOV@nornik.ru
M. V. Glibovets, Chief Engineer at the Talnakh Concentrator, e-mail: Glibovetsmv@nornik.ru
D. O. Midyukov, Principal Specialist at the Science and Technology Directorate, e-mail: MidyukovDO@nornik.ru

Реферат

Copper concentrate filtration station constitutes an initial stage in the production circuit of the Copper Plant, and maintaining the required throughput is crucial. Concentrate slurries from Talnakh and Norilsk Concentrators go to the filtration station, where industrial slurry products are also introduced in the production cycle. The filtration station is responsible for two key processes – thickening and filtering. Incoming slurry goes through two consecutive stages of thickening and the thickened product is then filtered. Due to increased performance targets, ceramic filters experience higher loads. Because of it, the established wash modes fail to maintain the necessary permeability of the filter membranes. Brown deposit can be regularly found on the ceramic filtering elements that significantly affects their permeability leading to emergency change-outs. In the course of the study, researchers found what causes the brown deposit on the surface of filter plates and how it forms. A study was conducted that looked at the applicability of reagents for the regeneration of filtering elements. Application of sulphuric acid was found to be the optimum solution. Further studies helped determine the concentration of sulphuric acid solution necessary to remove the deposit. Thus, it is proposed to use decopperized electrolyte from the copper electrowinning plant for filter plate regeneration. The best technical solution was also found. Thus, it is reasonable to use a separate wash tank to take a filter apart before removing the deposit. The industrial tests conducted demonstrated that the regeneration efficiency of the proposed process can be as high as 97%.
Other contributors to this research include A. V. Egorov, V. V. Velichko and O. Yu. Kokoev.

Ключевые слова Filtration, ceramic vacuum filters, filtering elements, regeneration of filter plates, copper concentrate slurry, sulphuric acid solution, iron metahydroxide, decopperized electrolyte.
Библиографический список

1. Bondar V. V., Burtovoy A. G., Krasnyi B. L., Rubtsov P. N. Operation of new generation disk vacuum filters with ceramic filtering elements. Tsvetnye Metally. 2004. No. 8. pp. 9–12.
2. Krasnyi B. L., Bondar V. V. Disk vacuum filters with ceramic filtering elements: Current status and prospective application. Tsvetnye Metally. 2007. No. 4. pp. 23–27.
3. Lan Ying Jiang, Li Na. Membrane-Based Separations in Metallurgy: Principles and Applications. Elsevier, 2017. 300 p.
4. Courtney A. Young. SME Mineral Processing and Extractive Metallurgy Handbook. Society for Mining, Metallurgy & Exploration. 2019. 2203 p.
5. Lebedev N. M., Zhirnova T. I., Voronin O. V. Intensified regeneration of ceramic SS-45 filters at Nornickel’s Norilsk Concentrator. Proceedings of the 4th conference of CIS concentration experts. 19–21 March 2003. Moscow : MISiS, 2003. p. 117.
6. Averina Yu. M., Zvereva O. V. Regeneration of ceramic membranes at a functioning plant: Process evaluation. Uspekhi v khimii i khimicheskoy tekhnologii. 2017. Vol. 31, No. 5. pp. 34–36.
7. Zemlyanskiy M. A., Ermakov S. A. KDF-75 ceramic vacuum filters: Design analysis. Education. Science. Production: 9th International Youth Forum. Belgorod, 1–10 October 2017. Belgorod : Belgorodskiy gosudarstvennyi tekhnicheskiy universitet imeni V. G. Shukhova, 2017. pp. 1265–1268.
8. Krasnyi A. B., Korolev M. N., Zimbovskiy I. G., Kruglov A. V. Method of ceramic filter element regeneration and composition for implementation thereof. Patent RF, No. 2739755. Applied: 26.02.2020. Published: 28.12.2020. Bulletin No. 1.
9. Sutherland K., Chase G. Filters and Filtration Handbook 5th Edition. Elsevier Science, 2008. 520 p.
10. Stovpenko A. S., Narizhnykh V. Yu., Lozovaya S. Yu. Ceramic disk vacuum filters: Performance analysis. Mezhdunarodnyi studencheskiy nauchnyi vestnik. 2015. No. 3-1. pp. 81–85.
11. Dudoladov V. V., Erkin V. M. Use of nuclear gamma resonance to understand how iron corrosion products form in alkaline solutions. Basic and Applied Problems of Physics: Proceedings of the 10th International Science and Technology Conference. 20–22 November 2017. Saransk : Mordovskiy gosudarstvennyi pedagogicheskiy institut imeni M. E. Evsevieva, 2017. pp. 55–59.
12. Popov V. V., Gorbunov A. I., Levina E. F. Regularities behind generation of nanocrystalline iron(III) oxyhydroxides as a result of neutral oxidation of iron(II) compounds. Zhurnal neorganicheskoy khimii. 2010. Vol. 55, No. 7. pp. 1063–1069.
13. Butenko A. M., Sincheskul O. L., Loboyko V. O., Markova N. B. Extraction of iron metahydroxides and their generation during STK catalyst production process. Vostochno-Evropeyskiy zhurnal peredovykh tekhnologiy. 2009. Vol. 5, No. 5. pp. 17–21.
14. Hrstka T., Gottlieb P., Skala R., Breiter K. Automated mineralogy and petrology – applications of TESCAN Integrated Mineral Analyzer (TIMA).

15. Velyaev Yu. O., Pokintelitsa N. I., Prokopenko I. A. Understanding the physico-chemical surface properties of iron metahydroxides obtained from reactive and mineral raw materials. The Scientific Heritage. 2021. No. 65–2. pp. 24–29.
16. Shabani N., Javadi H., Jafarizadeh-Malmiri H., Mirzaie J., Sadeghi A. Potential application of iron oxide nanoparticles synthesized by co-precipitation technology as a coagulant for water treatment in settling tanks. Mining, Metallurgy & Exploration. 2021. Vol. 38. pp. 269–276.

Language of full-text русский
Полный текст статьи Получить
Назад